C410&411 Lab. Syllabus

Instrumental Analysis

Sections K121/122



Instructor: Dr. Kasem K. Kasem e mail : kkasem@iuk.edu

Office : Room 236B Science Building

Phone : (765) 455-9245 Fax: (765) 455-9310

website : http:// www.iuk.edu/faculty/kkasem/kasemwebpage.htm



Text: D. A. Skoog, F. J. Holler, and T. A. Nieman

" PRINCIPLES OF INSTRUMENTAL ANALYSIS" fifth edition.



Lab Manual: IUPUI Lab Manual.



Lab.# Location Subject Date Lect. # Topic to be covered
1,

1-15

 IUK,SM Solvent

Properties

 01/14

01/16

 1

2

 Chapt. 1 Introduction

Chapt. 2 Elect. Comp.& Circuits

2,

1-22

 IUK, KC

Purdue Labs

 Elementary electronics 01/21

01/23

 .......

3

 No Class

Chapt. 3. Operational Amplifiers

3,

1-29

 IUK, KC

Purdue Labs

 Elementary electronics 01/28

01/30

 4

5

 Chapt. 4. Digital Electronics.

Chapt. 5. Signals & Noise.

4,

2-5

 IUK Chauret Lab Optical analy 02/4

02/6

 6

7

 Chapt. 6. Intro. to Spec. methods & Quiz 1

Chapt. 7/8. Optical Instru.& Spect

5.

2-12

 Hayns

Internat.

 Atomic Absorption 02/11

02/13

 8

9

 Chapt.9 Atom. Absorp.

Chapt. 10/11 Atomic Mass spec

6,

2-19

 Delco Electronics X-Ray

Analysis

 02/18

02/20

 10

11

 Chapt. 12. Atomic X-Ray Spectro.

Quiz 2, Chapt. 13. Introd.to UV

7,

2-26

 IUK lab UV analysis

of 3 comp.

 02/25

02/27

 12

13

 Review

Test 1

8,

3-5

 IUK lab FTIR

Spectroscop.

 03/4

03/6

 14

15

 Chapt. 14. Application of UV-VIS

Chapt.16 /17 Intro/Appl of IR

9,

3-12

 Hayns

Internat.

 Scan. Elect.

Microscope

 03/11

03/13

 16

17

 Chapt.20/ Molec. Mass Spect

Chapt 21/ Surface Spect

10 No Lab 03/18

03/20

 No

Classes

Spring Recess

11,

3-26

 IUK labs ISE/ CV 03/25

03/27

 18

19

 Quiz 3. Chapt.22 Electroanal

Chapt. 23 Potentio.

Lab.# Location Subject Date Lect. #

Topic to be covered
12,

4-1

 IUK labs. CV 03/31

04/3

 20

21

 Chapt. 25 Voltammetry

Chapt. 26 Intro to Chromatography

13,

4-9

 IUK lab GasChrom. (Finkler) 04/8

04/10

 22

23

 Chapt.27 Gas Chromatog. Chapt.28 HPLC
14,

4-16

 Delco Electro TGA 04/15

04/17

 24

25

 Quiz 4. Chapt. 31 Thermal anal

Review

15,

4-23

 IUK labs Calorimetric

measurem.

 04/22

04/24

 26

27

 Test 2

Special Project.(Calorimeters)

16,

4-30

 IUK labs Cunductivty

measurem.

 04/29

05/1

 28

29

 Special Project. ( Conductometric)

Review



05/10

30		 Review

Final Exam